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A 1:1 adduct between 2,2-bis­(chloro­di­methyl­stannyl)­propane and di­methyl sulfoxide

✍ Scribed by Mandolesi, Sandra ;Studentkowski, Marc ;Preut, Hans ;Mitchell, Terence


Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
199 KB
Volume
57
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.004 A Ê Disorder in solvent or counterion R factor = 0.026 wR factor = 0.050 Data-to-parameter ratio = 35.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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A 1:1 adduct between bis­(chloro­di­meth
✍ Mandolesi, Sandra ;Schürmann, Markus ;Preut, Hans ;Mitchell, Terence 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 248 KB

Single-crystal X-ray study T = 291 K Mean '(N±C) = 0.004 A Ê R factor = 0.027 wR factor = 0.063 Data-to-parameter ratio = 25.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Chloro­[N,N′-di­methyl-N,N′-bis(2-pyridy
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The title vanadium complex, [VClO(C 16 H 22 N 4 )]ClO 4 , of the tetradentate ligand N,N H -dimethyl-N,N H -bis(2-pyridylmethyl)ethane-1,2-diamine was obtained from air oxidation of a mixture of the ligand and VCl 3 in wet methanol.