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9,10,11,12-Tetrachloro-12b-hydroxy-2,12c-dimethyl-3a,5,6,12c-tetrahydrothiazalo[4,5-c][1,4]oxazepino[5,4-a]isoindol-8-one monohydrate

✍ Scribed by Fun, Hoong-Kun ;Teh, Jeannie Bee-Jan ;Chen, Da-Qing ;Xu, Jian-Hua

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 286 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807016674

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## Abstract Trimerization of butadiene in the presence of Ni(0) affords (1__E__,5__E__,9__E__)‐cyclododeca‐1,5,9‐triene **1** (__ttt__‐CDT), (1__E__,5__E__,9__Z__)‐cyclododeca‐1,5,9‐triene **2** (__ttc__‐CDT), and other isomers/oligomers. After optimization of reaction conditions, [^14^C~6~‐3,4,7,8