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9-(2-Phenyl­ethyl)-6-(2-thienyl)-9H-purine

✍ Scribed by Mazumdar, Pooja Anjali ;Das, Amit Kumar ;Bakkestuen, Anne Kristin ;Gundersen, Lise-Lotte ;Bertolasi, Valerio

Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
237 KB
Volume
57
Category
Article
ISSN
1600-5368

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The title compound, C 13 H 10 ClN 5 O 2 , crystallizes with two molecules in the asymmetric unit. These are connected by ®ve hydrogen bonds, viz. three NÐHÁ Á ÁN interactions, two longer C OÁ Á ÁÁHÐN interactions, bifurcated at the O atom, and a CÐHÁ Á ÁN contact.

Synthesis of 9-[(2-chloro-6-fluorophenyl
Synthesis of 9-[(2-chloro-6-fluorophenyl) [14C]methyl]-9H-purine-6-amine (arprinocid) and 9-[(2,6-dichlorophenyl) [14C]methyl]-9H-purine-6-amine
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The synthesis of 9-[(2-chloro-6-fluorophenyl)methyl]-9g-purin-6-amine (arprinocid, a coccidiostat candidate) and 9-[(2,6-dichlorophenyl)methyl]-9~-purin-6-amine labeled with carbon-14 in the benzylic methylene carbon of each of these is described. Introduction of the carbon-14 label leading to the f