✦ LIBER ✦

8-Hydroxyquinolinium–dibromosuccinate–dibromosuccinic acid (2/1/2)

✍ Scribed by Li, Dai-Xi ;Xu, Duan-Jun ;Xu, Yuan-Zhi

Publisher: International Union of Crystallography
Year: 2005
Tongue: English
Weight: 493 KB
Volume: 61
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536805001704

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.014 A Ê R factor = 0.064 wR factor = 0.170 Data-to-parameter ratio = 13.4

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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From an aqueous solution of racemic 2,3-dibromosuccinic acid and (__R__)-1-phenylethanamine, crystals of the title compound, C~8~H~12~N^+^·0.5C~4~H~2~Br~2~O~4~ ^2−^·0.5C~4~H~4~Br~2~O~4~·H~2~O, were obtained in almost quantitative yield. The structure contains both enantiomers of the starting materia

8-Hydro­xy­quinolinium–di­bromo­succinate–di­bromo­succinic acid (2/1/2)

✦ Synopsis

8-Hydroxyquinolinium–dibromosuccinate–dibromosuccinic acid (2/1/2)