𝔖 Bobbio Scriptorium
✦   LIBER   ✦

8-Chloro-6-(3-di­methyl­amino­propyl­amino)-11H-pyrido­[2,3-b][1,4]­benzodiazepine

✍ Scribed by Dupont, Léon ;Eyrolles, Laurence ;Evrard, Guy ;Delarge, Jacques ;Liégeois, Jean-François

Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
254 KB
Volume
58
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

8-Methyl-6-(4-methyl­piperazin-1-yl)-11H
8-Methyl-6-(4-methyl­piperazin-1-yl)-11H-pyrido­[2,3-b][1,4]­benzodiazepine
✍ Spirlet, Marie-Rose ;Graulich, Amaury ;Liégeois, Jean-Francois 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 240 KB

The conformation of the title compound, C 18 H 21 N 5 , is very similar to that observed in other diaryldiazepine structures such as clozapine and clozapine dihydrobromide. NÐHÁ Á ÁH hydrogen-bond interactions result in the formation of a dimer.

2-[2-(2,6-Di­methyl­phenyl­amino)­phenyl
2-[2-(2,6-Di­methyl­phenyl­amino)­phenyl­methyl­ene­amino]-1,3-diiso­propyl­benzene
✍ Gao, Haiyang ;Wu, Qing ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 176 KB

The ortho-disubstituted aromatic ring in the title compound, C 27 H 32 N 2 , is twisted by 76.1 (1) with respect to the isopropylsubstituted ring and by 89.3 (1) with respect to the methylsubstituted ring. The amino N atom is linked intramolecularly to the imino N by a hydrogen bond [NÁ Á ÁN = 2.686

8-Chloro-5-(4-methyl­piperazin-1-yl)-11H
8-Chloro-5-(4-methyl­piperazin-1-yl)-11H-pyrido­[2,3-b][1,5]­benzoxazepine. Erratum
✍ Dupont, Léon ;Liégeois, Jean-François 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 78 KB

In the paper by Dupont & Lie  geois [Acta Cryst. (2003), E59, o1962±o1963.], there is an error in the chemical name given in the title. The correct title is `8-Chloro-5-(4-methylpiperazin-1yl)pyrido[2,3-b][1,5]benzoxazepine'.