## Abstract 4,9βDimethoxynaphtho[2,3β__b__]furan 9 was obtained in 91% yield __via__ the reductive methylation of naphtho[2,3β__b__]furanβ4,9βdione 2. After treatment of 9 with butyllithium, the mixture was allowed to react with __N,N__βdimethylacetamide, followed by oxidization with cerium(IV) dia
7,9-Dimethyl-3-phenylnaphtho[1,2-b]furan-4,5-dione
β Scribed by Shen, Yudong ;Tian, Yuan-Xin ;Bu, Xian-Zhang
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 1024 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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The title compound, C 15 H 20 O 4 , also known as dihydrohelenalin, is a drug obtained from a Chinese plant. It contains a seven-membered ring in a chair conformation and two fivemembered rings in twist conformations. The crystal packing involves O-HΓ Γ ΓO hydrogen bonds. ## Related literature Fo
In the title compound, C~24~H~25~N~3~O~5~S, both the pyrrolidine and dihydropyran rings adopt envelope conformations, and are __cis__-fused. The tosyl group is equatorially attached to the pyrrolidine ring. The glide-related molecules are linked by CβH...O hydrogen bonds, forming a __C__(6) chain al