7-Isopropylidenebenzo-8,9,10-trinorbornadiene, C14H14
✍ Scribed by Galloy, J. ;Watson, W. H.
- Book ID
- 114501339
- Publisher
- International Union of Crystallography
- Year
- 1983
- Tongue
- English
- Weight
- 317 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0108-2701
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## Abstract The synthesis of the title compound (5) is described. Treatment of mitomycin C with sodium methoxide gave decarbamoyl mitomycin C (2). Reaction with acetic anhydride in methanol yielded N1a‐acetyl‐mitomycin C (3). Treatment with [^14^C]phosgene in the presence of N,N‐dimethylaniline yie
## Abstract trans‐7,8‐Dihydrobenzo[a]pyrene‐7,8‐diol‐7‐^14^C (VI) and (±)‐7α,8β‐dihydroxy‐9β,10β‐epoxy‐7,8,9,10‐tetrahydrobenzo[a]‐pyrene‐7‐^14^C (VII) were prepared at a specific activity of 53.9 mCi/mmole by a multi‐step synthetic sequence using K^14^CN as the labeled precursor. The overall radio