5,5-dimethyl-1,3-dioxan-4-ol as orthogonally protected equivalent of 2,2-dimethyl-3-hydroxypropanal
β Scribed by N. Z. Yagafarov, R. F. Valeev, R. F. Bikzhanov, E. I. Iginasheva, M. S. Miftakhov
- Book ID
- 111958252
- Publisher
- SP MAIK Nauka/Interperiodica
- Year
- 2012
- Tongue
- English
- Weight
- 192 KB
- Volume
- 48
- Category
- Article
- ISSN
- 1070-4280
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π SIMILAR VOLUMES
In the structure of the title compound, C 14 H 20 BrNO 5 , at 90 (2) K, the isoxazole is an axial substituent of the chair conformation dimethyldioxanyl ring. There is an antiparallel arrangement of the isoxazole rings with an oxygen to ring centroid distance of 3.402 (6) A Λ.
Single-crystal X-ray study T = 297 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.076 wR factor = 0.204 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.