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500 MHz NMR characterization of synthetic bombesin and related peptides in DMSO-d6 by two-dimensional techniques

✍ Scribed by Carlo Di Bello; Luigia Gozzini; Mauro Tonellato; Maria Grazia Corradini; Gabriella D'Auria; Livio Paolillo; Enrico Trivellone

Book ID: 115920330
Publisher: Elsevier Science
Year: 1988
Tongue: English
Weight: 811 KB
Volume: 237
Category: Article
ISSN: 0014-5793
DOI: 10.1016/0014-5793(88)80177-7

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The proton nmr characterization of bombesin (BBS) and of two peptide fragments corresponding to the (1-6) and (6-14) sequences has been carried out at 500 MHz in dimethyl sulfoxide (DMSO-d,) using two-dimensional (2D) homo and 'H-13C hetermorrelated techniques. All resonances in the nmr spectra have