𝔖 Bobbio Scriptorium
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(−)-5-endo,6-exo-Dihydroxycamphene

✍ Scribed by Spencer, S. A. ;Trotter, J.

Book ID
114526602
Publisher
International Union of Crystallography
Year
1979
Weight
188 KB
Volume
35
Category
Article
ISSN
0567-7408

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A convenient, high-yield synthesis of N-Boc-7-azabicyclo[2.2.1]hept-5-en-2-one (7) was developed by SmI 2 -mediated desulfonylation of 6. Thus, 5-endo-, 5-exo-, 6-endo-, and 6-exo-hydroxylated epibatidine analogues 2a,b and 3a,b were synthesized from 7 by using a Pd(PPh 3 ) 4 -catalyzed reductive He