𝔖 Bobbio Scriptorium
✦   LIBER   ✦

4b,4c,9b,9c-Tetrahydro-4b,4c,9b,9c-tetrachlorocyclobuta[1,2-a:3,4-a′]diindene-5,10-dione

✍ Scribed by Zhang, Shu-Sheng ;Zhang, Min ;Xu, Jian-Hua ;Li, Xue-Mei ;Fun, Hoong-Kun


Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
319 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.002 A Ê R factor = 0.029 wR factor = 0.084 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


📜 SIMILAR VOLUMES


4,4,6,8-Tetramethyl-2-tosylpyrrolo[3,4-c
✍ Chinnakali, K. ;Jayagopi, M. ;Sudha, D. ;Raghunathan, R. ;Fun, Hoong-Kun 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 1013 KB

In the title compound, C~20~H~25~N~3~O~5~S, the pyrrolidine ring is __trans__-fused to the dihydropyran ring. The pyrrolidine ring adopts a twist conformation and the dihydropyran ring is in an envelope conformation. The tosyl group is attached to the pyrrolidine ring in a biaxial position and its b