ChemInform Abstract: Synthesis of 2,4-Di
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Edward C. Taylor; James E. Dowling; Beena Bhatia
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Article
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2010
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John Wiley and Sons
⚖ 33 KB
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## Synthesis of 2,4- 6,7,8,9,9methanopyrimido[4,azocine. -Optimization of direct annulation of triaminopyrimidine (I) with cyclohexenone (II) is achieved using acetic acid as solvent in a screw-capped pressure tube that is heated at 120 • C for 18 hours. Compound (VII) as prototype, its derivative