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4,6,12,14-Tetra-tert-butyl-17-N-(6-methyl­pyridin-2-yl)-8,16-dioxa-17-aza­tetra­cyclo­[7.7.1.02,7.010,15]hepta­deca-2,4,6,10,12,14-hexa­ene methanol solvate

✍ Scribed by Xu, Li ;Kim, Youngmee ;Qi, Xin ;Kim, Sung-Jin

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
419 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The molecule of the title compoumd, C 37 H 52 N 2 O 3 , exhibits a propeller-like conformation, influenced by one intramolecular C-HÁ Á ÁN and four intramolecular C-HÁ Á ÁO hydrogen bonds. In the crystal structure, there are four weak C-HÁ Á Á interactions.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.047 wR factor = 0.159 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.