4,4-di methyl-5α-cholesta-8,14-dien-3β-ol A new precursor of cholesterol in mammalian tissues
✍ Scribed by A. Fiecchi; L. Canonica; A. Scala; F. Cattabeni; E. Grossi Paoletti; R. Paoletti
- Book ID
- 118934774
- Publisher
- Elsevier Science
- Year
- 1969
- Tongue
- English
- Weight
- 175 KB
- Volume
- 8
- Category
- Article
- ISSN
- 0024-3205
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The X-ray crystal structure of 3~-(p-bromobenzoyloxy)-5~-cholesta-8,14-diene (space group P21, a = 10.698 ,/~, b = 9.487 .~, c = 15.024 A, ~ = 96.05 °, Z = 2) was determined by the heavy atom method and refined to R = 0.075. This heavy atom derivative was synthesized from 5~-cholesta-8,14-dien-31~-o
## Abstract A sensitive, selective, precise, and robust high‐performance thin‐layer chromatography method was developed and validated for analysis of two new recently isolated sterols, 4α‐methyl‐24β‐ethyl‐5α‐cholesta‐14,25‐dien‐3β‐ol (**1**) and 24β‐ethylcholesta‐5,9(11),22__E__‐trien‐3β‐ol (**2**)