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4,4′-Bipyridyl–2-chloro-4-nitrobenzoic acid (1/2)

✍ Scribed by Gotoh, Kazuma ;Ishida, Hiroyuki


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
480 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


In the crystal structure of the title 1:2 cocrystal, C~10~H~8~N~2~·2C~7~H~4~ClNO~4~, the two components are held together by short O—H...N hydrogen bonds. The pyridine rings of the bipyridyl molecule are twisted by 27.90 (5)° with respect to each other. The 1:2 units are connected by C—H...O hydrogen bonds, forming a centrosymmetric supramolecular ring.


📜 SIMILAR VOLUMES


3-Cyano­pyridine–2-chloro-4-nitro­benzoi
✍ Ishida, Hiroyuki ;Fukunaga, Takeo 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 221 KB

Single-crystal X-ray study T = 300 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.119 Data-to-parameter ratio = 16.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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