𝔖 Bobbio Scriptorium
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(4-Oxo-3,4-dihydroquinazolin-3-yl)methyl piperidine-1-carbodithioate

✍ Scribed by She, Neng-Fang ;Huang, Wei


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
916 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


In the title compound, C 15 H 17 N 3 OS 2 , the piperidine ring adopts a chair conformation. Weak intermolecular C-HÁ Á ÁO hydrogen bonds link the molecules into chains along the c axis and further stability is provided by offsetstacking interactions [centroid separations = 3.73 (2)-3.78 (2) A ˚] involving the aromatic rings.


📜 SIMILAR VOLUMES


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## Abstract The cyclization of phenacyl anthranilate has been studied with the aim to develop the synthesis of 2‐(2′‐aminophenyl)‐4‐phenyloxazole. However, a different course of the reaction than expected was observed. 2‐Phenyl‐2‐hydroxymethyl‐4‐oxo‐1,2,3,4‐tetrahydroquinazoline (**3a**) was formed

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Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.004 A Ê R factor = 0.044 wR factor = 0.098 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.