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4-Ethyl-5-(2-hydroxy­phenyl)-2H-1,2,4-triazole-3(4H)-thione

✍ Scribed by Dege, Necmi ;Özdemir, Namık ;Çetin, Ahmet ;Cansız, Ahmet ;Şekerci, Memet ;Dinçer, Muharrem

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
327 KB
Volume
61
Category
Article
ISSN
1600-5368

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3-(2-Hydro­xy­phenyl)-4-phenyl-1H-1,2,4-
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The title molecule, C 14 H 11 N 3 OS, is non-planar. The phenyl and hydroxyphenyl rings form dihedral angles of 69.08 (9) and 24.57 (9) , respectively, with the ®ve-membered 2,4-dihydro-1,2,4-triazole ring. The molecules form centrosymmetric dimers through NÐHÁ Á ÁS hydrogen bonds, with an NÁ Á ÁS d

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The title compound, C 15 H 13 N 3 S, was prepared by the reaction of 1-(2-chloroethyl)benzene with hydrazine and phenyl isothiocyanate. Packing is stabilized by N-HÁ Á ÁS intermolecular hydrogen bonds and C-HÁ Á Á interactions.

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✍ Dinçer, Muharrem ;Özdemir, Namık ;Çetin, Ahmet ;Cansız, Ahmet ;Şekerci, Memet 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 290 KB

In the title compound, C 8 H 8 N 4 OS, the planar triazole ring is effectively coplanar with the benzene ring, which facilitates the formation of three intramolecular interactions N-HÁ Á ÁS (leading to a thione tautomer in the solid state), O-HÁ Á ÁN and C-HÁ Á ÁN. Intermolecular N-HÁ Á ÁS interacti

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✍ Yıldırım, Sema Öztürk ;Akkurt, Mehmet ;Koparır, Metin ;Cansız, Ahmet ;Şekerci, M 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 260 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.002 A Ê R factor = 0.036 wR factor = 0.084 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.