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3-(2-Hydro­xy­phenyl)-4-phenyl-1H-1,2,4-triazole-5(4H)-thione

✍ Scribed by Genç, Sadık ;Dege, Necmi ;Çetin, Ahmet ;Cansız, Ahmet ;Şekerci, Memet ;Dinçer, Muharrem

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
319 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title molecule, C 14 H 11 N 3 OS, is non-planar. The phenyl and hydroxyphenyl rings form dihedral angles of 69.08 (9) and 24.57 (9) , respectively, with the ®ve-membered 2,4-dihydro-1,2,4-triazole ring. The molecules form centrosymmetric dimers through NÐHÁ Á ÁS hydrogen bonds, with an NÁ Á ÁS distance of 3.279 (2) A Ê . In addition, the molecule contains one OÐHÁ Á ÁN and one CÐHÁ Á Á%(phenyl) intramolecular interactions. The dimers are connected through weak intermolecular CÐHÁ Á Á%(hydroxyphenyl) interactions into chains in the a direction.

📜 SIMILAR VOLUMES

3-Benzyl-4-phenyl-1H-1,2,4-triazole-5(4H
3-Benzyl-4-phenyl-1H-1,2,4-triazole-5(4H)-thione
✍ Jian, Fangfang ;Bai, Zhengshuai ;Xiao, Hailian ;Li, Kai 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 124 KB

The title compound, C 15 H 13 N 3 S, was prepared by the reaction of 1-(2-chloroethyl)benzene with hydrazine and phenyl isothiocyanate. Packing is stabilized by N-HÁ Á ÁS intermolecular hydrogen bonds and C-HÁ Á Á interactions.

3-(2-Furyl)-4-(4-methoxy­phenyl)-1H-1,2,
3-(2-Furyl)-4-(4-methoxy­phenyl)-1H-1,2,4-triazole-5(4H)-thione
✍ Yıldırım, Sema Öztürk ;Akkurt, Mehmet ;Koparır, Metin ;Cansız, Ahmet ;Şekerci, M 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 260 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.002 A Ê R factor = 0.036 wR factor = 0.084 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

3-Benzyl-4-(4-chloro­phenyl)-1H-1,2,4-tr
3-Benzyl-4-(4-chloro­phenyl)-1H-1,2,4-triazole-5(4H)-thione
✍ Öztürk, Sema ;Akkurt, Mehmet ;Cansız, Ahmet ;Koparır, Metin ;Şekerci, Mehmet ;He 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 228 KB

In the title molecule, C 15 H 12 ClN 3 S, the dihedral angles made by the substituted phenyl and benzyl rings with the triazole ring are 81.39 (10) and 63.59 (10) , respectively. The crystal structure is stabilized by NÐHÁ Á ÁS, CÐHÁ Á ÁCl and CÐHÁ Á Á% interactions.