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4-Alkoxy-1-phenylphosphacyclohexadiene → 1-Alkoxy-1-phenyl-λ5-phosphorin Rearrangement

✍ Scribed by Prof. Dr. Gottfried Märkl; Dipl.-Chem. Rainer Liebl; Alois Hüttner

Publisher: John Wiley and Sons
Year: 1978
Tongue: English
Weight: 319 KB
Volume: 17
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.197805281

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A well stirred solution of 3-methyllumiflavin~"1 (1.50g, 5.5 mmol) and N,N-dimethylpropargylamine (4.6 g, 55.0 mmol) in 0.1 M phosphate buffer (600 ml, pH 7.7) was illuminated under argon for 30 hours with a 170 W mercury high-piessure lamp (HERAEUS, Hanau; pyrex cooling jacket). The brown precipita