The title compound, C~15~H~14~F~2~N~2~O~2~S, was synthesized by the reaction of 1-(2,4-difluorophenyl)ethanone and 4-methylbenzenesulfonohydrazide in ethanol under reflux. The crystal structure is stabilized mainly through intermolecular N—H...O hydrogen bonds. The C=N—N group displays a __trans__ c
4-(2,4-Difluorophenyl)-2-(N-methylcarbamoyl)phenyl acetate
✍ Scribed by Zhong, Guang-Xiang ;Li, Jian ;Zheng, Ren-Hua ;Zhao, Kun
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 292 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.063 wR factor = 0.225 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.041 wR factor = 0.100 Data-to-parameter ratio = 19.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.059 wR factor = 0.147 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.