4-(1H-Indol-3-yl)-2,6-bis(4-methoxyphenyl)pyridine
✍ Scribed by Tu, Shujiang ;Li, Tuanjie ;Fang, Fang
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 194 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 27 H 22 N 2 O 2 , was synthesized by the reaction of indole-3-carbaldehyde with 4-methoxyacetophenone and ammonium acetate in glycol under microwave irradiation. X-ray analysis reveals that NÐHÁ Á ÁN hydrogen bonds link the molecules into zigzag chains along [011].
📜 SIMILAR VOLUMES
In the title molecule, C 22 H 18 N 4 O, all of the rings and the indole system are individually planar. In the crystal structure, molecules are linked by intermolecular N-HÁ Á ÁO hydrogen bonds, forming infinite chains running along the [001] direction.
In the title compound, C 30 H 24 ClNO 3 S, the phenylsulfonyl, chlorophenyl and methoxyphenyl rings are each almost perpendicular to the indole ring system. The crystal packing shows centrosymmetrically related pairs of molecules. Intermolecular C-HÁ Á ÁO interactions are present.