{4-[(1-Naphthyl)vinyl]phenyl}di-p-tolylamine
✍ Scribed by Cao, Xiao-Dan ;Liu, Dong-Zhi ;Zhou, Xue-Qin ;Sun, Shao-Feng
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 136 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 32 H 23 Cl 2 N, was synthesized via the Ullmann reaction. The orientations of the three aromatic rings attached to the vinyl group are determined by the sp 2 state of the vinyl C atoms. The crystal packing is stabilized by weak CÐHÁ Á Á% interactions.
The crystal structure of the title compound, C 28 H 23 NO 2 S, reveals that the phenylsulfonyl ring and the adjacent benzene ring are anti, with no evidence of stacking.
The title compound, C 22 H 19 FN 2 , was prepared by reacting phenylhydrazine with 1-(4-fluorophenyl)-3-(p-tolyl)prop-2enone. The pyrazoline ring forms a dihedral angle of 5.2 (3) with the phenyl ring, 8.8 (1) with the fluorophenyl ring and 80.7 (2) with the p-tolyl ring.