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(+)-(3R)-N-Hydro­xy-2-[(S)-ethoxy(4-methoxy­phenyl)­phospho­ryl]-1,2,3,4-tetra­hydro­iso­quinoline-3-carbox­amide

✍ Scribed by Kurokawa, Kiriko ;Kanehisa, Nobuko ;Sawa, Masaaki ;Kondo, Hirosato ;Kai, Yasushi

Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
221 KB
Volume
57
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.004 A Ê R factor = 0.041 wR factor = 0.102 Data-to-parameter ratio = 10.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.044 wR factor = 0.124 Data-to-parameter ratio = 7.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 29 H 27 NO 7 , has a non-planar con®guration. The methoxycarbonylmethyl group exhibits an E con®guration. The crystal structure is stabilized by intermolecular OÐHÁ Á ÁO and CÐHÁ Á ÁO contacts.