3,6-Bis(4-methoxybenzyloxy)pyridazine
✍ Scribed by Hu, Fang-Zhong ;Zhang, Min ;Song, Hai-Bin ;Zou, Xiao-Mao ;Yang, Hua-Zheng
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 153 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
In the crystal structure of the title compound, C 20 H 20 N 2 O 4 , the molecules are linked by a weak intermolecular C-HÁ Á ÁN hydrogen bond. The molecule has crystallographic twofold rotation symmetry.
📜 SIMILAR VOLUMES
In the title compound, C 15 H 12 Cl 2 O 3 , the isovanillin group makes a dihedral angle of 3.12 (12) with the dichlorobenzene ring. Intermolecular C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
An anhydrous ethanol solution of 4-benzyloxy-3-methoxybenzaldehyde (2.42 g, 10 mmol) was added to an anhydrous ethanol
The title compound, C 21 H 19 N 3 O 3 , was prepared by the reaction of 4-benzyloxy-3-methoxybenzaldehyde and isonicotinohydrazide. The vanillin group makes dihedral angles of 27.88 (7) and 58.94 (6) with the planes of the pyridine and phenyl rings, respectively. A weak intermolecular C-HÁ Á ÁN hydr