2-Benzyloxy-3-methoxybenzaldehyde (benzyl-o-vanillin)
✍ Scribed by Al-Douh, Mohammed H. ;Hamid, Shafida A. ;Osman, Hasnah ;Ng, Shea-Lin ;Fun, Hoong-Kun
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 311 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the title compound, C 15 H 12 Cl 2 O 3 , the isovanillin group makes a dihedral angle of 3.12 (12) with the dichlorobenzene ring. Intermolecular C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
An anhydrous ethanol solution of 4-benzyloxy-3-methoxybenzaldehyde (2.42 g, 10 mmol) was added to an anhydrous ethanol
The title compound, C 21 H 19 N 3 O 3 , was prepared by the reaction of 4-benzyloxy-3-methoxybenzaldehyde and isonicotinohydrazide. The vanillin group makes dihedral angles of 27.88 (7) and 58.94 (6) with the planes of the pyridine and phenyl rings, respectively. A weak intermolecular C-HÁ Á ÁN hydr