The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.
3,5-Bis{4-[(benzimidazol-1-yl)methyl]phenyl}-4H-1,2,4-triazol-4-amine and its one-dimensional polymeric complex with HgCl2
✍ Scribed by Li, Yan-an ;Liu, Qi-Kui ;Ma, Jian-Ping ;Dong, Yu-Bin
- Book ID
- 111924794
- Publisher
- International Union of Crystallography
- Year
- 2012
- Tongue
- English
- Weight
- 775 KB
- Volume
- 68
- Category
- Article
- ISSN
- 0108-2701
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Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.084 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 15 H 10 Cl 2 N 4 O 5 S, is a potent new herbicide. Intramolecular C-HÁ Á ÁO and intermolecular C-HÁ Á ÁO and C-HÁ Á ÁN hydrogen bonds seem to be effective in the crystal structure. The intermolecular hydrogen bonds link the molecules into a three-dimensional network.
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.003 A R factor = 0.043 wR factor = 0.113 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.