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3,4,5-Trimethoxy-1-methylbenzene

✍ Scribed by Li, Jian ;Liang, Zu-Pei ;Wan, Ai-Yu ;Zeng, Wu-Lan

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
495 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

Experimental

Crystal data C 10 H 14 O 3 M r = 182.21 Monoclinic, P2 1 =n a = 13.902 (11) A b = 8.123 (7) A c = 18.021 (14) A = 98.883 (14) V = 2011 (3) A ˚3 Z = 8 Mo K radiation = 0.09 mm À1 T = 294 (2) K 0.26 Â 0.24 Â 0.22 mm Data collection Bruker SMART CCD area-detector diffractometer Absorption correction: multi-scan (SADABS; Bruker, 1997) T min = 0.978, T max = 0.981 10097 measured reflections 3556 independent reflections 2019 reflections with I > 2(I) R int = 0.045 Refinement R[F 2 > 2(F 2 )] = 0.045 wR(F 2 ) = 0.146 S = 1.00 3556 reflections 243 parameters

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In the title compound, C 18 H 18 O 4 , the dihedral angle between the benzene rings is 9.07 (7) . Intermolecular C-HÁ Á ÁO interactions form chains along the c axis. The crystal structure is further stabilized by C-HÁ Á Á interactions.