3,3′-Didecyl-5,5′-bis(4-phenylquinolin-2-yl)-2,2′-bithienyl
✍ Scribed by Benedict, Jason B. ;Kaminsky, Werner ;Tonzola, Christopher J.
- Book ID
- 104481638
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 514 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 130 K Mean '(C±C) = 0.007 A Ê Disorder in main residue R factor = 0.067 wR factor = 0.151 Data-to-parameter ratio = 14.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.
The title compound, C~26~H~36~N~2~O~6~P~2~, possesses a crystallographically imposed inversion centre. The molecules are linked into a one-dimensional structure along the __c__ axis by a centrosymmetric system of weak C—H...O hydrogen bonds.
The title compound, C 21 H 18 N 6 S 2 , crystallizes with one halfmolecule in the asymmetric unit; a twofold rotation axis passes through the central C atom. The triazine ring makes a dihedral angle of 10.65 (2) with the benzene ring.