3′-(Methylsulfanyl)biphenyl-4-carbonitrile
✍ Scribed by Zhang, Zhi-Qiang ;Hu, Zhi-Zhi ;Wang, Cui-Ping ;Yan, Jing-Bo ;He, Ren
- Book ID
- 104492282
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 253 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 22 H 21 ClN 4 O, is used as an intermediate for the synthesis of biologically active compounds. Geometric parameters are in the usual ranges. The packing is stabilized by O-HÁ Á ÁN hydrogen bonding.
## Abstract The synthesis of 6‐methylsulfanyl‐2,4‐dithioxo‐1,2,3,4‐tetrahydropyrimidine‐5‐carbonitrile **4** is described. Compound **4** was reacted with various alkylants. The reaction with chloroacetic acid derivatives results in the formation of thieno[2,3‐__d__]pyrimidines **8**. When methyl i