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3-Ethyl-2,5-dimethylpyrazine, a component of the trail pheromone of the antMessor bouvieri

✍ Scribed by B. D. Jackson; P. J. Wright; E. D. Morgan

Book ID: 105410361
Publisher: Springer
Year: 1989
Tongue: English
Weight: 325 KB
Volume: 45
Category: Article
ISSN: 1420-682X
DOI: 10.1007/bf01952041

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Hydrogenation of 4-cholesten-3-one (1) with tritium gas over palladium black in pyridine afforded [P-4,5-SH]-cholestan-3-one (2a). Tritium NMR showed that there was a mixture of tritiated compounds formed, 2a-2c; the latter two containing small amounts of protium substitution. Tritium NMR also indi