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3-(6-Methoxybenzothiazol-2-yldiazenyl)-1-methyl-2-phenyl-1H-indole

✍ Scribed by Hökelek, Tuncer ;Seferoğlu, Zeynel ;Şahin, Ertan ;Kaynak, Filiz Betül

Book ID
104490883
Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
202 KB
Volume
63
Category
Article
ISSN
1600-5368

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1-Methyl-2-phenyl-3-(1,3,4-thia­diazol-2
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In the molecule of the title compound, C 17 H 13 N 5 S, all of the rings are individually planar. The thiadiazole and phenyl rings form dihedral angles of 7.67 (4) and 49.77 (5) , respectively, with the indole ring system.

1-Methyl-2-phenyl-1H-indole
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In the structure of the title compound, C 15 H 13 N, the dihedral angle between the five-and the six-membered rings of the indole system is 1.19 (5) and the phenyl ring makes a dihedral angle of 46.09 (5) with the indole ring system.

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To a stirred solution of aluminium chloride (20 mmol) in dry tetrahydrofuran (100 ml), sodium azide (60 mmol) and 1-phenylsulfonyl-