Single-crystal X-ray study T = 298 K Mean (C-C) = 0.006 A Disorder in main residue R factor = 0.095 wR factor = 0.243 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
3-[(2-Hydroxy-5-nitrophenyl)amino]-2-benzofuran-1(3H)-one monohydrate
✍ Scribed by Odabaşoğlu, Mustafa ;Büyükgüngör, Orhan
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 295 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The crystal structure of the title compound, C~14~H~10~N~2~O~5~·H~2~O, is stabilized by inversion-related O—H...O and C—H...O intermolecular hydrogen bonds and also by π–π interactions. The dihedral angle between the phthalide group and the benzene ring is 51.45 (8)°.
📜 SIMILAR VOLUMES
In the title compound, C~17~H~12~ClN~3~O~5~, the benzene rings are twisted out of the central –C~ar~–C–C(–CN)–C(=O)–N–plane. The dihedral angles between this plane and the aromatic planes are 31.2 (4) and 4.8 (3)°. The C=C double bond is in an __E__ configuration.
Single-crystal X-ray study T = 298 K Mean (C-C) = 0.006 A R factor = 0.084 wR factor = 0.197 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 15 H 14 ClO 2 , the dihedral angle between the two benzene rings is 57.37 (12) .