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(2S)-1-(Benzoyl­thio­carbamo­yl)pyrrolidine-2-carboxylic acid monohydrate

✍ Scribed by Ngah, Nurziana ;Kassim, Mohammad B. ;Yamin, Bohari M.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
314 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 13 H 14 N 2 O 3 SÁH 2 O, the benzoyl group lies out of the plane of the N 2 CS thiourea unit, having a C carbonyl -N-C-S torsion angle of 119.4 (4) . The crystal structure is stabilized by N-HÁ Á ÁO, O-HÁ Á ÁO, C-HÁ Á ÁO and C-HÁ Á ÁS intermolecular hydrogen bonds, forming a twodimensional network.

📜 SIMILAR VOLUMES

(S)-Benzyl 2-[N-(5-chloropyridin-2-yl)ca
(S)-Benzyl 2-[N-(5-chloropyridin-2-yl)carbamoyl]pyrrolidine-1-carboxylate
✍ He, Long 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 394 KB

In the title compound, C~18~H~18~ClN~3~O~3~, the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the phenyl ring and the pyridine ring is 28.30 (7)°. The crystal packing is stabilized by N—H...O and C—H...O hydrogen bonding.