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29Si NMR in LC–NMR analysis of silicones

✍ Scribed by Vratislav Blechta; Jan Sýkora; Jiří Hetflejš; Stanislav Šabata; Jan Schraml

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
127 KB
Volume
44
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

It is demonstrated using a practical example that indirect detection of ^29^Si NMR signals is sufficiently sensitive in LC–NMR stop‐flow arrangement to analyze mixtures of siloxane polymers. New cryogenic probes with better signal‐to‐noise ratio will turn this version of LC–NMR into a routine method for analysis of siloxane polymers. Copyright © 2005 John Wiley & Sons, Ltd.

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