280. A synthesis of 2-(2 : 3-dimethoxyphenyl)cyclohexanone
✍ Scribed by Bergmann, Ernst D. ;Pappo, Raphael ;Ginsburg, David
- Book ID
- 111939219
- Publisher
- The Royal Society of Chemistry
- Year
- 1950
- Weight
- 279 KB
- Category
- Article
- ISSN
- 0368-1769
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📜 SIMILAR VOLUMES
The title compound, C 12 H 13 NO 3 , adopts its enol tautomeric form and crystallizes with two molecules in the asymmetric unit, with similar conformations. In the crystal structure, molecules interact via O-HÁ Á ÁN hydrogen bonds, leading to infinite chains. ## Related literature For background
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.034 wR factor = 0.101 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 19 H 18 ClN 3 O 5 S 2 , which is a representative of a class of inactive acetolactate synthase inhibitors, the dihedral angle between the two aromatic groups is 85.9 (1) .