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276. The preparation of dl-asparagine and dl-aspartic acid

✍ Scribed by Cocker, Wesley

Book ID: 118280736
Publisher: The Royal Society of Chemistry
Year: 1940
Weight: 269 KB
Category: Article
ISSN: 0368-1769
DOI: 10.1039/jr9400001489

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A synthesis of the title compound from /13Clparaformaldehyde and [15N)ammonium chloride V f 8 ethyl 2-(1 ,3-/2-13Cldithianyl) acetate 3a is described. Ethyl/3-13C13-oxopropanoate derived in sl'tu from 3a was converted by a stepwise Strecker procedure to DL-[ 2-13C,15Nlaspartic acid 7a.