𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2,3:5,6-Di-O-iso­propyl­idene-2-C-hydro­xymethyl-d-talono-1,4-lactone

✍ Scribed by Shallard-Brown, Howard A. ;Harding, Christopher C. ;Watkin, David J. ;Soengas, Raquel ;Skytte, Ulla P. ;Fleet, George W. J.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
282 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

2,2′:5,6-Di-O-iso­propyl­idene-2-C-hydro
2,2′:5,6-Di-O-iso­propyl­idene-2-C-hydro­xymethyl-d-talono-1,4-lactone
✍ Harding, Christopher C. ;Watkin, David J. ;Cowley, Andrew R. ;Soengas, Raquel ;S 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 410 KB

A second crystalline diacetonide, the title compound, C 13 H 20 O 7 , has been isolated from the sequential treatment of d-tagatose with aqueous sodium cyanide, followed by acetone in the presence of acid. Structural ambiguities with regard to the size of both the lactone and ketal rings are resolve

3-Azido-3-deoxy-2,2′:5,6-di-O-iso­propyl
3-Azido-3-deoxy-2,2′:5,6-di-O-iso­propyl­idene-2-C-hydro­xmethyl-d-gulono-1,4-lactone
✍ Harding, Christopher C. ;Shallard-Brown, Howard ;Watkin, David J. ;Soengas, Raqu 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 897 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.108 Data-to-parameter ratio = 9.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

5-Amino-5-deoxy-2-C-hydroxy­methyl-2,3-O
5-Amino-5-deoxy-2-C-hydroxy­methyl-2,3-O-iso­propyl­idene-d-talono-1,5-lactam
✍ Ameijde, Jeroen van ;Cowley, Andrew R. ;Fleet, George W. J. ;Nash, Robert J. ;Si 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

The title compound, C 10 H 17 NO 6 , was prepared by carrying out three S N 2 displacements on a branched sugar derivative, one of which was not planned. Its crystal structure was determined to con®rm the identity and stereochemistry of the product.

2-Azido-2-deoxy-3,4-O-iso­propyl­idene-2
2-Azido-2-deoxy-3,4-O-iso­propyl­idene-2-C-methyl-d-ribono-1,5-lactone
✍ Punzo, Francesco ;Watkin, David J. ;Jenkinson, Sarah F. ;Cruz, Filipa P. da ;Fle 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 250 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.004 A Ê R factor = 0.045 wR factor = 0.102 Data-to-parameter ratio = 11.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.