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2′,3′-Di­phenyl-4′-p-tolyl­spiro­[iso­thia­chroman-3,5′-isoxazolidin]-4(2H)-one

✍ Scribed by Bennani, Brahim ;Filalibaba, Bouchra ;El-Fazazi, Ahmed ;Houari, Ghali Al ;Bilit, Najib ;Kerbal, Abdelali ;El-Bali, Brahim ;Bolte, Michael


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
216 KB
Volume
58
Category
Article
ISSN
1600-5368

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5-(2-Chloro­phenyl)-2-p-tolyl-1,3,4-thia
✍ Huang, Hua-Ming ;Yu, Hai-Tao ;Chen, Pei-Li ;Meng, Ji-Ben 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 237 KB

The title compound, C 15 H 11 ClN 2 S, has been prepared by the reaction of Lawesson's reagent with N-(2-chlorobenzoyl)-N H -(4-methylbenzoyl)hydrazine, under microwave irradiation and in the absence of solvent. It crystallizes with two molecules per asymmetric unit and X-ray analysis reveals that t