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2,3-Dimethylenebicyclo[2.2.0]hexane and its cycloreversion to 2,3-dimethylenecyclohexa-1,3-diene

✍ Scribed by Chang, Chiu-Shan; Bauld, Nathan L.


Book ID
126092510
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
239 KB
Volume
94
Category
Article
ISSN
0002-7863

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Table 1. Selected physical properties of ( 5 a ) and (56) "C-NMR (in CDCl3, T M S internal) c-1 109.2 C-CN 97.4, 98.9, 102.0 c-4 108.9 c -5 c-1 ' 124.5 c -2 , c-3' 131.1 IR ( K B r ) [cm-'1 C=N 2210 Cyclopropene [5] 1898, 1550 UV(CH3CN) [ n m l (log&) 240 (4.61), 278 (4.23) 'H-NMR (100 MHz, CDClj, T