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2-Methyl-1-(methyl­sulfin­yl)naphtho[2,1-b]furan

✍ Scribed by Choi, Hong Dae ;Woo, Hyun Mi ;Seo, Pil Ja ;Son, Byeng Wha ;Lee, Uk

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
157 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 14 H 12 O 2 S, was prepared by the oxidation of 2-methyl-1-(methylsulfanyl)naphtho[2,1-b]furan using m-chloroperbenzoic acid. The crystal structure contains aromaticstacking, C-HÁ Á ÁO and C-HÁ Á Á interactions.

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1-Methyl­sulfinyl-2-phenyl­naphtho[2,1-b
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The title compound, C~21~H~16~N~2~O~5~, was synthesized by the reaction of 2-naphthol with methyl cyanoacetate and 3-nitrobenzaldehyde in ethanol under microwave irradiation. The pyran ring adopts a boat conformation.