𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2-Fluoro-N-[7-fluoro-3,4-di­hydro-2-methyl-3-oxo-4-(prop-2-ynyl)-2H-1,4-benzoxazin-6-yl]­benz­amide

✍ Scribed by Hou, Zhong-Ke ;Ao, Cong-Cong ;Song, Jian ;Chen, Li-Gong

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
176 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.054 wR factor = 0.137 Data-to-parameter ratio = 12.5

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

3-(3-Fluoro­benz­yl)-2-thioxo-2,3,5,6-te
3-(3-Fluoro­benz­yl)-2-thioxo-2,3,5,6-tetra­hydro­pyrimidin-4(1H)-one
✍ Yu, Chen-Xia ;Yao, Chang-Sheng ;Tu, Shu-Jiang ;Wang, Xiang-Shan ;Jiang, Hong 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 165 KB

In the title molecule, C~11~H~11~FN~2~OS, conformational disorder is observed in the tetrahydropyrimidine ring and both components adopt half-chair conformations. In the crystal structure, the molecules are linked by C—H...O and N—H...S hydrogen bonds, forming a sheet-like structure parallel to the

3-(2,3-Di­hydro-1,5-di­methyl-3-oxo-2-ph
3-(2,3-Di­hydro-1,5-di­methyl-3-oxo-2-phenyl­pyrazol-4-yl­imino)-4,4,4-tri­fluoro-1-(2-thienyl)­butane-1,2-dione
✍ Wang, Jin-Ling ;Yu, Ming ;Su, Xiu-Mei ;Miao, Fang-Ming 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 259 KB

The title compound, C 19 H 14 F 3 N 3 O 3 S, is built up from pyrazolinone, thiophene, phenyl rings and tri¯uoropropanedicarbonyl moieties. Examination of the ÐC N and ÐC O bond lengths reveals that there is no electron delocalization over the molecule.

N-{3-Cyano-1-[2,6-di­chloro-4-(tri­fluor
N-{3-Cyano-1-[2,6-di­chloro-4-(tri­fluoro­methyl)­phenyl]-1H-pyrazol-5-yl}benz­amide
✍ Zhong, Ping ;Yang, Zhiping ;Li, Shuyan ;Tang, Riyuan 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 336 KB

The title compound, C 18 H 9 Cl 2 F 3 N 4 O, is a tricyclic amide with an overall U-shape. NÐHÁ Á ÁN hydrogen bonds generate linear chains which extend along the a axis.