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3-(2,3-Di­hydro-1,5-di­methyl-3-oxo-2-phenyl­pyrazol-4-yl­imino)-4,4,4-tri­fluoro-1-(2-thienyl)­butane-1,2-dione

✍ Scribed by Wang, Jin-Ling ;Yu, Ming ;Su, Xiu-Mei ;Miao, Fang-Ming


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
259 KB
Volume
58
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, C 19 H 14 F 3 N 3 O 3 S, is built up from pyrazolinone, thiophene, phenyl rings and tri¯uoropropanedicarbonyl moieties. Examination of the ÐC N and ÐC O bond lengths reveals that there is no electron delocalization over the molecule.


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(2RS,3RS)-2,3-Di­methyl-1,4-bis(3,4,5-tr
✍ Hu, Qingping ;Ma, Mingliang ;Shi, Jixian ;Li, Yan ;Zhou, Hongyu 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 167 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.042 wR factor = 0.120 Data-to-parameter ratio = 15.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.