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2-Deoxy-D-ribose. V. 1 Synthesis of the Two Anomeric 9-(2-Deoxy-D-ribofuranosyl)-adenines through 5-Benzoyl-2-deoxy-D-ribose Diisopropyl Dithioacetal

✍ Scribed by Pedersen, Christian; Fletcher, Hewitt G.

Book ID: 127147806
Publisher: American Chemical Society
Year: 1960
Tongue: English
Weight: 263 KB
Volume: 82
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01504a045

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The title compound 2-Deoxy-3,5-di-O-benzoyl-2,2-difluoro-D-ribose (17), was synthesised from D-glucose and from D-mannose. The key steps of the synthesis from D-glucose are obtaining the 3,3-difluoropyranose 9 by reacting the ulose 7 with DAST. and their conversion into the difluorofuranoside 17 by