(2-Chlorophenyl)diphenylphosphine
✍ Scribed by Williams, Michael L. ;Noack, Cassandra L. ;Saverin, Rodney J. ;Healy, Peter C.
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 213 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.039 wR factor = 0.115 Data-to-parameter ratio = 19.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.041 wR factor = 0.088 Data-to-parameter ratio = 21.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, [Cu 4 Br 4 (C 17 H 14 NP) 4 ]Á6CH 2 Cl 2 , the centrosymmetric Cu 4 Br 2 group is in a slightly distorted plane, forming a shuttle-like structure. Each of the Cu I ions is coordinated by two Br, N and P atoms, with metal±metal bonds between neighbouring Cu atoms.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.031 wR factor = 0.072 Data-to-parameter ratio = 16.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.