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2-chloro-2-thio-1,3,2-oxoazaphosphacyclohexane and its derivatives

✍ Scribed by O. V. Kil'disheva; A. Puzerauskas; E. Ya. Pervova

Book ID
112434121
Publisher
Springer
Year
1968
Tongue
English
Weight
140 KB
Volume
17
Category
Article
ISSN
1573-9171

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In the title compound, C 14 H 10 Cl 2 N 2 OS, the geometric parameters do not show unusual features. The thiocarbonyl and carbonyl groups are almost coplanar with the chlorophenyl ring, as reflected by the torsion angles of 0.7 (3) and À5.8 (3) , respectively. The structure exhibits inter-and intram

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The phenyl and benzoyl groups in the title molecule, C~14~H~11~ClN~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The molecular conformation is stabilized by an N—H...O hydrogen bond and the crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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✍ Saeed, Aamer ;Ritch, Jamie S. ;Parvez, Masood 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 224 KB

The structure of the title compound, C 15 H 9 ClO 2 S, has a thioisocoumarin unit and a substituted phenyl group that are twisted at a dihedral angle of 33.40 ( 6) with respect to one another. In addition to weak O-HÁ Á ÁS interactions, C-HÁ Á ÁS/O/Cl-type interactions that stabilize the structure a