2-(Benzoylmethylsulfanyl)-6-methoxy-1H-benzimidazole
✍ Scribed by Lynch, Daniel E. ;McClenaghan, Ian
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 148 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.061 wR factor = 0.126 Data-to-parameter ratio = 12.7
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The title compound was synthesized by adding benzohydrazide (0.136 g, 1 mmol) to an absolute ethanol solution (30 ml) containing 3-[bis(methylsulfanyl)methylene]dihydro-6-methyl-3H-pyran-2,4-dione (0.232 g, 1 mmol). The mixture was stirred for 5.5 h at room temperature. The product was obtained by s
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