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2-Amino-6-methoxy-4-(4-methoxy­phenyl)-9,10-di­hydro-4H-benzo­[f]­chromene-3-carbo­nitrile

✍ Scribed by Yu, Chen-Xia ;Shi, Da-Qing ;Wang, Xiang-Shan ;Zhuang, Qi-Ya


Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
346 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, C 22 H 20 N 2 O 3 , was synthesized by the reaction of 4-methoxybenzaldehyde, 7-methoxy-2-tetralone and malononitrile in the presence of triethylbenzylammonium chloride in an aqueous medium. X-ray analysis reveals that the pyran ring and the fused six-membered ring adopt boat and skew-boat conformations, respectively.


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3-Amino-1-(3,4-methyl­enedioxy­phenyl)-9
✍ Yu, Chen-Xia ;Shi, Da-Qing ;Wang, Xiang-Shan ;Zhuang, Qi-Ya 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 365 KB

The title compound, C 22 H 18 N 2 O 4 , was synthesized by the reaction of 7-methoxy-2-tetralone and 3,4-methylenedioxybenzylidenemalononitrile in the presence of triethylbenzylammonium chloride in an aqueous medium. X-ray analysis reveals that the pyran ring and the fused six-membered ring adopt bo