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2-{5-[N-(4-tert-Butyl­benz­yl)carbamo­yl]-3-phenyl-1H-pyrazol-1-yl}acetic acid

✍ Scribed by Ge, Yan-Qing ;Xia, Yong ;Dong, Wen-Liang ;Wei, Fang ;Zhao, Bao-Xiang

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
112 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C~23~H~25~N~3~O~3~, all bond lengths and angles show normal values. The dihedral angles between the rings of the pyrazole and the unsubstituted and tert-butyl-substituted benzene rings are 8.6 (2) and 78.5 (3)°, respectively, while that between the two benzene rings is 76.6 (3)°.

📜 SIMILAR VOLUMES

5-Amino-4-(benzotriazol-1-yl­methyl)-1-p
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Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.003 A Ê R factor = 0.061 wR factor = 0.150 Data-to-parameter ratio = 16.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Synthesis and Characterization of Some 2
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In the title compound, C 29 H 25 NO 2 S 2 , the benzene rings of the phenylsulfonyl and the dimethylbenzyl substituents are almost perpendicular to the indole unit, whereas the dihedral angle between the phenyl rings of the phenylsulfanyl and phenylsulfonyl groups is 71.2 (1) . The molecules in the

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The title compound, C 20 H 21 NO, was obtained by the reaction of indole-3-carbaldehyde with 4-tert-butylbenzyl chloride and recrystallization of the product from ethanol. The indole ring system is nearly planar and makes a dihedral angle of 74.45 (3) with the plane of the 4-tert-butylphenyl ring.

4-{(2,4-Dichloro­phen­yl)[5-hydr­oxy-1-p
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The title compound, C 27 H 16 Cl 2 F 6 N 4 O 2 ÁH 2 O, was obtained by the reaction of 2,4-dichlorobenzaldehyde and 2-phenyl-5trifluoromethyl-2H-pyrazol-3-ol in aqueous media without any catalyst. In the crystal structure, both intra-and intermolecular hydrogen bonds are found.

1-tert-But­yl-3-(trifluoro­meth­yl)-1H-p
1-tert-But­yl-3-(trifluoro­meth­yl)-1H-pyrazol-5-yl 4-chloro­benzoate
✍ Li, Yang ;Li, Jiang-Sheng ;Huang, Peng-Mian ;Duan, Xue-Min ;Dong, Chuan-Ming ;Ze 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 101 KB

In the title compound, C 15 H 14 ClF 3 N 2 O 2 , the benzene and pyrazolyl rings form a dihedral angle of 15.9 (3) .