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2-(1H-Benzo-1,2,3-triazol-1-yl)-4,4-di­methyl-3-oxo-N-phenyl­pentane­thio­amide monohydrate

✍ Scribed by Xu, Liangzhong ;Yang, Shuanghua ;Qin, Yongqi ;Yang, Yaxun ;Huang, Yongwei

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
136 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 19 H 22 N 4 O 2 SÁH 2 O, was synthesized in order to search for new benzotriazole compounds with high bioactivity. There are some intermolecular hydrogen-bond interactions in the crystal structure, providing stabilization.

Experimental

The title compound was prepared by reaction of 1-(1Hbenzo[1,2,3]triazol-1-yl)-3,3-dimethylbutan-2-one (4.34 g, 0.02 mol),

📜 SIMILAR VOLUMES

Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-
Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-4H-1,2,4-triazol-3-yl] di­sulfide
✍ Pan, Fu-You ;Yang, Jian-Guo ;Chen, Ding-Ben ;Huang, Ling 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.