The title compound 3 was obtained during the rearrangement of isoxazol-5-yl hydrazine 1 to 1 -aminopyrazolone 2 at \(115^{\circ}\). X-ray analysis of the corresponding benzylidene derivative allowed us to achieve the structure assignment.
(1S)-Benzyl 3-methyl-5-oxo-4-phenylhydrazono-4,5-dihydro-1H-pyrazole-1-dithiocarboxylate
β Scribed by Liu, Yong-Hong ;Zhao, Yue ;Liu, Xiao-Lan ;Tong, Ben-Wan ;Ye, Jun
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 424 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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π SIMILAR VOLUMES
The molecules of the title compound, C~22~H~18~N~2~, are connected by NβH...N hydrogen bonds, forming cyclic dimers. These dimers are linked by CβH...Ο hydrogen bonds involving the phenyl rings as acceptors.
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